AFM tecniques

 

AFMs can be utilized to scan a sample in two different modes: contact mode or tapping mode, according to the interatomic force vs. distance (tip-to sample) curve.

In the contact zone, the cantilever is held few angstroms from the sample surface and the interatomic force between the cantilever and the sample is repulsive. AFM tip makes soft "physical contact" with the sample. - Contact operative mode. The tip is attached to the end of a cantilever with a low spring constant, lower than the effective spring constant holding the atoms of the sample together. The magnitude of the total force exerted on the sample varies from 10-8 to the more typical operating range of 10-7 to 10-6N.
In the non-contact zone, the cantilever is held on the order of tens to hundreds of angstroms from the sample surface and the interatomic force between the cantilever and the sample is attractive  - Non-contact operative mode.

The AFM cantilever is vibrated near the surface of the sample obtaining little or no contact between the tip and the sample. The magnitute of the total force is very low, generally about 10-12N: this low force is advantageous for studying soft or elastic samples. The system vibrates a stiff cantilever near its resonant frequency (typically from 100 to 400 kHz) with an amplitude of a few tens to hundreds of angstroms.
Both the operative regimes provide a means of measuring sample topography.

 

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